SOLVED: The Tolman cone angles of PPh3 and P(4-MeCsH3)3 are both 145°, but that of P(2-MeCsH4)3 is 194°. Explain the difference in the angle values and draw a sketch of the two phosphines to illustrate your answer. [Fe(CO)5] has absorptions at 2025 and 2000 cm-1, whereas [Fe(CO)(PPh3)2] has absorptions at 1944, 1886, and 1881 cm-1. Explain the influence of the phosphine ligand on the decrease of IR frequency.
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